Undergraduate Instrumental Analysis

This book provides a comprehensive guide to modern analytical techniques in environmental science, covering UPLC and hyphenated techniques, sampling, sample handling, storage, and preparation, and expanding coverage of surface analysis.

Format: Hardback
Length: 996 pages
Publication date: 31 July 2023
Publisher: Taylor & Francis Ltd

This comprehensive book provides detailed coverage of the latest developments in ultra-performance liquid chromatography (UPLC) and hyphenated techniques. It offers a thorough exploration of sampling, sample handling, sample storage, and sample preparation, ensuring a comprehensive understanding of these critical aspects in analytical chemistry. Additionally, the book expands its coverage to include in-depth discussions on surface analysis, providing readers with a comprehensive understanding of the techniques and applications used in this field. With its authoritative content and practical approach, this book is an essential resource for researchers, students, and professionals in analytical chemistry and related disciplines.

Introduction:
Ultra-performance liquid chromatography (UPLC) has emerged as a powerful tool in analytical chemistry, offering high resolution, speed, and sensitivity for the analysis of a wide range of compounds. Hyphenated techniques, which combine UPLC with other analytical methods such as mass spectrometry or infrared spectroscopy, have further enhanced the capabilities of UPLC. This comprehensive book aims to provide detailed coverage of the latest developments in UPLC and hyphenated techniques, covering topics such as sampling, sample handling, sample storage, and sample preparation.
Sampling:
Sampling is a critical step in any analytical process, and UPLC and hyphenated techniques have revolutionized the way samples are collected and prepared. In UPLC, small sample volumes are required, which can be achieved through microsampling techniques such as solid-phase microextraction (SPME) or microfluidics. Hyphenated techniques, on the other hand, allow for the simultaneous analysis of multiple samples, providing a more efficient and cost-effective approach.
Sample Handling:
Sample handling is another critical aspect of analytical chemistry, and UPLC and hyphenated techniques have introduced new methods and technologies to improve the efficiency and accuracy of sample preparation. In UPLC, automated sample preparation systems are commonly used, which can handle large volumes of samples and perform multiple steps in a single run. Hyphenated techniques, such as solid-phase microextraction followed by mass spectrometry, have also been developed to enhance the selectivity and sensitivity of sample analysis.
Sample Storage:
Sample storage is an important consideration in analytical chemistry, as it can affect the accuracy and reliability of the results. UPLC and hyphenated techniques have introduced new storage solutions, such as solid-state containers or cryogenic storage, which can preserve the integrity of the samples and prevent degradation. Hyphenated techniques, such as UPLC-MS/MS, have also been developed to analyze complex samples that require multiple analytical methods.
Sample Preparation:
Sample preparation is a critical step in analytical chemistry, as it can affect the accuracy and sensitivity of the results. UPLC and hyphenated techniques have introduced new methods and technologies to improve the efficiency and selectivity of sample preparation. In UPLC, solid-phase extraction techniques are commonly used to pre-concentrate the analytes before injection into the chromatographic system. Hyphenated techniques, such as UPLC-MS/MS, have also been developed to analyze complex samples that require multiple analytical methods.
Surface Analysis:
Surface analysis is a growing field in analytical chemistry, and UPLC and hyphenated techniques have played a significant role in its development. In UPLC, surface-enhanced Raman spectroscopy (SERS) has been used to analyze the surface properties of materials, including drugs, biomaterials, and environmental samples. Hyphenated techniques, such as UPLC-SERS followed by mass spectrometry, have also been developed to identify and quantify the surface-bound compounds in complex samples.
Conclusion:
In conclusion, this comprehensive book provides detailed coverage of the latest developments in UPLC and hyphenated techniques, covering topics such as sampling, sample handling, sample storage, and sample preparation. It also expands its coverage to include in-depth discussions on surface analysis, providing readers with a comprehensive understanding of the techniques and applications used in this field. With its authoritative content and practical approach, this book is an essential resource for researchers, students, and professionals in analytical chemistry and related disciplines.

Weight: 2982g
Dimension: 221 x 288 x 55 (mm)
ISBN-13: 9781032036915
Edition number: 8 ed